ORGANIC
AND MACROMOLECULAR SYNTHESIS FACILITY
Publications from
the Internal Research Program
(publications as of 6/12/08)
Jumpstart Phase
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C. Edder, P. B. Armstrong,
K. B. Prado and J. M. J. Fréchet, "Synthesis
of Soluble Polymers Containing Pyrrole and Thiophene Moieties",
Abstracts of Papers of the American Chemical Society (2005).
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C. Edder, P. B. Armstrong, K. B. Prado and
J. M. J. Fréchet, "Benzothiadiazole-
and Pyrrole-Based Polymers Bearing Thermally Cleavable Solubilizing
Groups as Precursors for Low Bandgap Polymers", Chemical
Communications 2006,
3 (2006). [pdf]
Operations Phase
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F. Svec and C. G. Huber, "Monolithic Materials: Promises,
Challenges, Achievements", Analytical Chemistry 78 (7),
8 (2006). [pdf]
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F. Svec, "Less Common Applications of Monoliths: Preconcentration
and Solid-Phase Extraction", Journal of Chromatography
B 841,
13 (2006). [pdf]
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J. Germain, J. Hradil, J. M. J. Fréchet and F. Svec, "High
Surface Area Nanoporous Polymers for Reversible Hydrogen Storage",
Chemistry of Materials 18 (18), 6 (2006). [pdf]
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M. Slater, M. Snauko, F. Svec and J. M. J.
Fréchet, ""Click
Chemistry" In the Preparation of Porous Polymer-Based Particulate
Stationary Phases for Mu-Hplc Separation of Peptides and Proteins",
Analytical Chemistry 78 (14), 6 (2006). [pdf]
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F. Svec and S. Eeltink, "Recent Advances in the Control of
Morphology and Surface Chemistry of Porous Polymer-Based Monolithic
Stationary Phases and Their Application in Cec", Electrophoresis 28 (1-2),
137-147 (2007). [ pdf]
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T. B. Stachowiak, D. A. Mair, T. G. Holden,
L. J. Lee, F. Svec and J. M. J. Fréchet, "Hydrophilic Surface Modification
of Cyclic Olefin Copolymer Microfluidic Chips Using Sequential
Photografting", Journal of Separation Science 30 (7),
5 (2007). [pdf]
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S. Eeltink, L. Geiser, F. Svec and J. M. J.
Fréchet, "Optimization
of the Porous Structure and Polarity of Polymethacrylate-Based
Monolithic Capillary Columns for the Lc-Ms Separation of Enzymatic
Digests", Journal of Separation Science 30 (17),
6 (2007). [pdf]
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Y. Liu, L. M. Klivansky, S. I. Khan and X.
Zhang, "Templated
Synthesis of Desymmetrized [2]Catenanes with Excellent Translational
Selectivity", Organic Letters 9, 4 (2007). [pdf]
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D. A. Mair, M. Rolandi, M. Snauko, R. Noroski,
J. M. J. Fréchet
and F. Svec, "Room Temperature Bonding for Plastic High Pressure
Microfluidic Chips", Analytical Chemistry 79 (13),
5 (2007). [pdf]
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Y. Liu, "Self-Assembled Ring-in-Ring Complexes from Metal–Ligand
Coordination Macrocycles and Β-Cyclodextrin", Tetrahedron
Letters 48 (22), 3 (2007). [pdf]
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J. Germain, J. M. J. Frechet and F. Svec, "Nanoporous Polymers
for Hydrogen Storage", Polym. Mat. Sci. Eng. 97,
272 (2007). [pdf]
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J. Germain, J. M. J. Fréchet and F. Svec, "Hypercrosslinked
Polyanilines with Nanoporous Structure and High Surface Area: Potential
Adsorbents for Hydrogen Storage", Journal of Materials
Chemistry 17,
8 (2007). [ pdf]
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J. Germain, J. M. J. Fréchet and F. Svec, "Nanoporous
Polymers for Reversible Hydrogen Storage", Polymeric Materials
Science and Engineering 97, 2 (2007). [pdf]
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Y. Liu, X. Zhang, L. M. Klivansky and G. Koshkakaryan, "Enhancing
the Reactivity of 1,2,3-Triazoles in ‘Click’ Macrocycles
by Face-to-Face Dibenzylammonium Ion Binding", Chemical
Communications 45,
3 (2007). [ pdf]
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F. Svec and T. B. Stachowiak, in Handbook of Capillary and
Microchip Electrophoresis and Associated Microtechniques,
edited by J. Landers (Taylor & Francis, Boca Raton, 2007),
pp. 1297-1326. [pdf]
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V. Augustin, T. B. Stachowiak, F. Svec and
J. M. J. Frechet, "Cec
Separation of Peptides Using Poly(Hexyl Acrlyate-Co-1,4-Butanediol
Diacrylate-Co-[2-(Acryloyloxy)Ethyl]Trimethyl Ammonium
Chloride) Monolithic Column", Electrophoresis in press (2008).
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P. A. Levkin, S. Eeltink, T. R. Stratton, R.
Brennen, K. Robotti, K. Killeen, F. Svec and J. M. J. Frechet, "Monolithic Porous
Polymer Stationary Phases in Polyamide Chips for the Fast High-Performance
Liquid Chromatography Separation of Proteins and Peptides",
J. Chromatography A in press (2008).
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F. Svec, "Stellan Hjerten's Contribution
to the Development of Monolithic Stationary Phases", Electrophoresis in
press (2008). [ pdf]
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L. Geiser, S. Eeltink, F. Svec and J. M. J.
Frechet, "In-Line
System Containing Porous Polymer Monoliths for Protein Digestion
with Immobilized Pepsin, Peptide Preconcentration and Nano-Liquid
Chhromatography Separation Coupled to Electrospray Ionization Mass
Spectroscopy", J. Chromatography A 1188,
88 (2008). [ pdf]
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F. Svec and J. Krenkova, "Rigid Pourous Polymer Monoliths
as Stationary Phases and Supports", LC-GC America 26 (2008). [pdf]
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F. Svec and A. A. Kurganov, "Less Common Applications of Monoliths
Iii: Gas Chromatography", J. Chromatography A 1184,
281 (2008). [ pdf]
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Y. Liu, A. Bruneau, J. He and Z. Abliz, "Palladium(Ii) Directed
Self Assembly of Dynamic Donor-Acceptor [2]Catenanes",
Organic Letters 10 (5), 765 (2008). [ pdf]
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